4,4'-bis-(carboxyl phenylazo)-dibenzo-18-crown-6

Base Information

Chemical Name:4,4'-bis-(carboxyl phenylazo)-dibenzo-18-crown-6
CAS No.:1312773-97-9
Molecular Formula:C₃₄H₃₂N₄O₁₀
Molecular Weight:656.649
Hs Code.:

Synonyms:4,4'-bis-(carboxyl phenylazo)-dibenzo-18-crown-6

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-bis-(carboxyl phenylazo)-dibenzo-18-crown-6

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Technology Process of 4,4'-bis-(carboxyl phenylazo)-dibenzo-18-crown-6

There total 1 articles about 4,4'-bis-(carboxyl phenylazo)-dibenzo-18-crown-6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.5%

: 14187-32-7
dibenzo-18-crown-6

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 1312773-97-9
4,4'-bis-(carboxyl phenylazo)-dibenzo-18-crown-6

Guidance literature:: 4-amino-benzoic acid; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 0.5h;

dibenzo-18-crown-6; In water; at 0 - 5 ℃; for 2h; aq. phosphate buffer;
DOI:10.1016/j.saa.2011.03.054

Reference yield:

: 1312773-97-9
4,4'-bis-(carboxyl phenylazo)-dibenzo-18-crown-6

: 14302-87-5
mercury ion

: 1312791-90-4
Hg(4,4'-bis(carboxyl phenylazo)-dibenzo-18-crown-6)⁽²⁺⁾

Guidance literature:: With acetic acid; sodium acetate; In water; dimethyl sulfoxide; aq. soln. of Hg(2+) and DMSO soln. of ligand in presence of acetate buffer (pH 5.0) stirred for 15 min; not isolated; detd. by UV-vis spectra;
DOI:10.1016/j.saa.2011.03.054