N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline hydrochloride

Base Information

Chemical Name:N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline hydrochloride
CAS No.:1441168-50-8
Molecular Formula:C₁₇H₂₄FN*ClH
Molecular Weight:297.844
Hs Code.:

Synonyms:N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline hydrochloride

Chemical Property:

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Technology Process of N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline hydrochloride

There total 8 articles about N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1441169-64-7
N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline

: 1441168-50-8
N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; at 20 ℃; for 2h;

Reference yield:

: 1439355-94-8
(E)-7-(isopropoxymethylene)-2,2-dimethylcycloheptanone

: 1441168-50-8
N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline hydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydroxide / water; ethanol / 9 h / Reflux

2: zinc(II) iodide / dichloromethane / 2 h / 20 °C

3: hydrogenchloride / tetrahydrofuran; water / 20 °C

4: thionyl chloride; pyridine / 2 h / 20 °C

5: diisobutylaluminium hydride / dichloromethane; hexane / 2 h / -78 °C / Inert atmosphere

6: acetic acid; sodium cyanoborohydride / methanol / 2 h / 20 °C

7: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

8: hydrogenchloride / diethyl ether / 2 h / 20 °C

With pyridine; hydrogenchloride; thionyl chloride; sodium hydride; diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; sodium hydroxide; zinc(II) iodide; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1439355-96-0
2,2-dimethyl-1-(trimethylsilyloxy)cycloheptanecarbonitrile

: 1441168-50-8
N-((7,7-dimethylcyclohept-1-enyl)methyl)-3-fluoro-N-methylaniline hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / tetrahydrofuran; water / 20 °C

2: thionyl chloride; pyridine / 2 h / 20 °C

3: diisobutylaluminium hydride / dichloromethane; hexane / 2 h / -78 °C / Inert atmosphere

4: acetic acid; sodium cyanoborohydride / methanol / 2 h / 20 °C

5: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

6: hydrogenchloride / diethyl ether / 2 h / 20 °C

With pyridine; hydrogenchloride; thionyl chloride; sodium hydride; diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide;