4-Isobutyl-2-methylbenzaldehyde

Base Information

Chemical Name:4-Isobutyl-2-methylbenzaldehyde
CAS No.:73206-60-7
Molecular Formula:C₁₂H₁₆O
Molecular Weight:176.258
Hs Code.:
European Community (EC) Number:811-502-1
DSSTox Substance ID:DTXSID001019624
Nikkaji Number:J3.496.248K

Synonyms:4-Isobutyl-2-methylbenzaldehyde;SCHEMBL17748247;4-isobutyl-2-methyl benzaldehyde;DTXSID001019624;73206-60-7

Suppliers and Price of 4-Isobutyl-2-methylbenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-Isobutyl-2-methylbenzaldehyde

Chemical Property:

Boiling Point:262℃ at 101.2kPa
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:176.120115130
Heavy Atom Count:13
Complexity:163

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=CC(=C1)CC(C)C)C=O

Technology Process of 4-Isobutyl-2-methylbenzaldehyde

There total 9 articles about 4-Isobutyl-2-methylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 73206-52-7
2-methyl-4-isobutylphenyl bromide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 73206-60-7
2-methyl-4-isobutylbenzaldehyde

Guidance literature:: 2-methyl-4-isobutylphenyl bromide; With magnesium; In tetrahydrofuran; at 70 - 85 ℃; Large scale;

N,N-dimethyl-formamide; In tetrahydrofuran; at 10 - 30 ℃; for 2h; Large scale;

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 5160-99-6
1-iso-butyl-3-methylbenzene

: 68102-28-3
2-isobutyl-4-methylbenzaldehyde

: 73206-60-7
2-methyl-4-isobutylbenzaldehyde

Guidance literature:: formaldehyd; 1-iso-butyl-3-methylbenzene; With hydrogenchloride; acetic acid; at 40 ℃; Inert atmosphere;

With hexamethylenetetramine; acetic acid; In ethanol; for 10h; Inert atmosphere; Reflux;

Reference yield:

: 5160-99-6
1-iso-butyl-3-methylbenzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 68102-28-3
2-isobutyl-4-methylbenzaldehyde

: 73206-60-7
2-methyl-4-isobutylbenzaldehyde

Guidance literature:: 1-iso-butyl-3-methylbenzene; With bromine; iodine; iron; at 10 - 20 ℃; for 7h; Large scale;

With magnesium; In tetrahydrofuran; at 70 - 85 ℃; Large scale;

N,N-dimethyl-formamide; In tetrahydrofuran; at 10 - 30 ℃; for 2h; Overall yield = 48 percent; Overall yield = 6260 g; Large scale;
DOI:10.1021/acs.oprd.0c00421