3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin

Base Information

• Chemical Name: 3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin
• CAS No.: 118210-62-1
• Molecular Formula: C₃₂H₂₆OS₂
• Molecular Weight: 490.69

Synonyms:3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin

Chemical Property of 3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin

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Technology Process of 3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin

There total 2 articles about 3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

2-(phenylthio)methylenetetralin-1-thione dimer (118210-61-0) + 1,3-diphenyl-propen-3-one (614-47-1) → 2-benzoyl-3,4,5,6-tetrahydro-3-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin (118210-63-2) + 3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin (118210-62-1)

Guidance literature:

In benzene; for 2h; Heating;

DOI:10.1246/bcsj.63.2540

Reference yield: 59.0%

2-(phenylthio)methylenetetralin-1-thione dimer (118210-61-0) + 1,3-diphenyl-propen-3-one (614-47-1) → 2-benzoyl-3,4,5,6-tetrahydro-3-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin (118210-63-2) + 3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin (118210-62-1)

Guidance literature:

In benzene; for 2h; Heating;

DOI:10.1246/cl.1988.1029

Reference yield: 90.0%

3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin (118210-62-1) → 3-benzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene (118210-64-3)

Guidance literature:

With sodium ethanolate; In benzene;

DOI:10.1246/bcsj.63.2540

upstream raw materials:

2-(phenylthio)methylenetetralin-1-thione dimer

1,3-diphenyl-propen-3-one

2-(phenylthio)methylenetetralin-1-thione dimer

Downstream raw materials:

3-benzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzochrysene

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