benzyl (S)-2-((S)-6-((S)-2-azido-3-methylbutanoyl)-5-isobutyl-4-oxo-1,3,6-oxadiazepan-3-yl)-3-methylbutanoate

Base Information

Chemical Name:benzyl (S)-2-((S)-6-((S)-2-azido-3-methylbutanoyl)-5-isobutyl-4-oxo-1,3,6-oxadiazepan-3-yl)-3-methylbutanoate
CAS No.:1303516-19-9
Molecular Formula:C₂₅H₃₇N₅O₅
Molecular Weight:487.599
Hs Code.:

Synonyms:benzyl (S)-2-((S)-6-((S)-2-azido-3-methylbutanoyl)-5-isobutyl-4-oxo-1,3,6-oxadiazepan-3-yl)-3-methylbutanoate

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Chemical Property of benzyl (S)-2-((S)-6-((S)-2-azido-3-methylbutanoyl)-5-isobutyl-4-oxo-1,3,6-oxadiazepan-3-yl)-3-methylbutanoate

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Technology Process of benzyl (S)-2-((S)-6-((S)-2-azido-3-methylbutanoyl)-5-isobutyl-4-oxo-1,3,6-oxadiazepan-3-yl)-3-methylbutanoate

There total 4 articles about benzyl (S)-2-((S)-6-((S)-2-azido-3-methylbutanoyl)-5-isobutyl-4-oxo-1,3,6-oxadiazepan-3-yl)-3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₉N₅O₆

: 1303516-19-9
benzyl (S)-2-((S)-6-((S)-2-azido-3-methylbutanoyl)-5-isobutyl-4-oxo-1,3,6-oxadiazepan-3-yl)-3-methylbutanoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja2023898

Reference yield:

: 1219453-07-2
(S)-2-((S)-2-azido-N-formyl-3-methylbutanamido)-4-methylpentanoic acid

: 1303516-19-9
benzyl (S)-2-((S)-6-((S)-2-azido-3-methylbutanoyl)-5-isobutyl-4-oxo-1,3,6-oxadiazepan-3-yl)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,6-dimethylbenzene-1-thiol / chloroform / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

2.1: acetic anhydride / propan-1-ol; dichloromethane / 0.08 h / -60 °C / Inert atmosphere

2.2: 3 h / -60 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylbenzene-1-thiol; acetic anhydride; trifluoroacetic acid; In propan-1-ol; dichloromethane; chloroform;
DOI:10.1021/ja2023898

Reference yield:

: 1219452-98-8
N₃-Val(CHO)Leu-Ot-Bu

: 1303516-19-9
benzyl (S)-2-((S)-6-((S)-2-azido-3-methylbutanoyl)-5-isobutyl-4-oxo-1,3,6-oxadiazepan-3-yl)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: formic acid / 4 h / 20 °C / Inert atmosphere

2.1: 2,6-dimethylbenzene-1-thiol / chloroform / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

3.1: acetic anhydride / propan-1-ol; dichloromethane / 0.08 h / -60 °C / Inert atmosphere

3.2: 3 h / -60 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylbenzene-1-thiol; formic acid; acetic anhydride; trifluoroacetic acid; In propan-1-ol; dichloromethane; chloroform;
DOI:10.1021/ja2023898