tert-butyl 4-methyl-5-oxo-3-phenyl-5,6-dihydropyridine-1(2H)-carboxylate

Base Information

Chemical Name:tert-butyl 4-methyl-5-oxo-3-phenyl-5,6-dihydropyridine-1(2H)-carboxylate
CAS No.:1372173-57-3
Molecular Formula:C₁₇H₂₁NO₃
Molecular Weight:287.359
Hs Code.:

Synonyms:tert-butyl 4-methyl-5-oxo-3-phenyl-5,6-dihydropyridine-1(2H)-carboxylate

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Chemical Property of tert-butyl 4-methyl-5-oxo-3-phenyl-5,6-dihydropyridine-1(2H)-carboxylate

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Technology Process of tert-butyl 4-methyl-5-oxo-3-phenyl-5,6-dihydropyridine-1(2H)-carboxylate

There total 3 articles about tert-butyl 4-methyl-5-oxo-3-phenyl-5,6-dihydropyridine-1(2H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 673-32-5
1-Phenylprop-1-yne

: 398489-26-4
tert-butyl 3-oxoazetidine-1-carboxylate

: 1372173-57-3
tert-butyl 4-methyl-5-oxo-3-phenyl-5,6-dihydropyridine-1(2H)-carboxylate

Guidance literature:: With bis(triphenylphosphine)nickel(II) chloride; zinc; In acetonitrile; at 80 ℃; for 20h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.5b01458

Reference yield: 81.0%

: 1372173-57-3
tert-butyl 4-methyl-5-oxo-3-phenyl-5,6-dihydropyridine-1(2H)-carboxylate

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; triphenylphosphine; In toluene; at 100 ℃; Inert atmosphere; Glovebox;

In toluene; at 100 ℃; for 6h;

Reference yield: 80.0%

: 673-32-5
1-Phenylprop-1-yne

: 398489-26-4
tert-butyl 3-oxoazetidine-1-carboxylate

: 1372173-57-3
tert-butyl 4-methyl-5-oxo-3-phenyl-5,6-dihydropyridine-1(2H)-carboxylate

: 1379664-27-3
C₁₇H₂₁NO₃

Guidance literature:: With nickel⁽⁰⁾(1,5-cyclooctadiene)2; triphenylphosphine; In 1,4-dioxane; at 90 ℃; for 17h; regioselective reaction; Inert atmosphere;
DOI:10.1002/chem.201200167