C₅₁H₇₃F₃O₁₂

Base Information

Chemical Name:C₅₁H₇₃F₃O₁₂
CAS No.:1360572-23-1
Molecular Formula:C₅₁H₇₃F₃O₁₂
Molecular Weight:935.129
Hs Code.:

C<sub>51</sub>H<sub>73</sub>F<sub>3</sub>O<sub>12</sub>

Synonyms:C₅₁H₇₃F₃O₁₂

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Chemical Property of C₅₁H₇₃F₃O₁₂

Chemical Property:

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Technology Process of C₅₁H₇₃F₃O₁₂

There total 18 articles about C₅₁H₇₃F₃O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1360572-21-9
C₄₁H₆₆O₁₀

: 20445-33-4,39637-99-5
(R)-methoxytrifluoromethylphenylacetyl chloride

: 1360572-23-1
C₅₁H₇₃F₃O₁₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 30 ℃; for 24h; Inert atmosphere;
DOI:10.1002/anie.201106762

Reference yield:

: 1360572-18-4
(2R,3R,4R)-2,4-dimethylhept-5-yn-1,3-diol

: 1360572-23-1
C₅₁H₇₃F₃O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridinium p-toluenesulfonate / dichloromethane / 1 h / Molecular sieve; Inert atmosphere

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 3.83 h / -78 - 20 °C / Inert atmosphere

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.58 h / -78 - -40 °C / Inert atmosphere

3.2: -40 - 20 °C / Inert atmosphere

4.1: boron trifluoride diethyl etherate / toluene / 0.5 h / -78 °C / Inert atmosphere

5.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 20 °C / Inert atmosphere

6.1: Schwartz's reagent / benzene / Inert atmosphere; Heating

6.2: -25 °C / Inert atmosphere

7.1: chromium dichloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); (R)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methanesulfonamide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / acetonitrile / 20 °C / Inert atmosphere

8.1: dmap; triethylamine / dichloromethane / 24 h / 30 °C / Inert atmosphere

With chromium dichloride; dmap; Schwartz's reagent; oxalyl dichloride; (R)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methanesulfonamide; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In hexane; dichloromethane; toluene; acetonitrile; benzene; 3.1: Swarts reaction / 7.1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1002/anie.201106762

Reference yield:

: 850479-61-7
(S)-pent-3-yn-2-yl methanesulfonate

: 1360572-23-1
C₅₁H₇₃F₃O₁₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: indium iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 17 h / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 13.58 h / 0 - 20 °C / Inert atmosphere

3.1: pyridinium p-toluenesulfonate / dichloromethane / 1 h / Molecular sieve; Inert atmosphere

4.1: diisobutylaluminium hydride / hexane; dichloromethane / 3.83 h / -78 - 20 °C / Inert atmosphere

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.58 h / -78 - -40 °C / Inert atmosphere

5.2: -40 - 20 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate / toluene / 0.5 h / -78 °C / Inert atmosphere

7.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 20 °C / Inert atmosphere

8.1: Schwartz's reagent / benzene / Inert atmosphere; Heating

8.2: -25 °C / Inert atmosphere

9.1: chromium dichloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); (R)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methanesulfonamide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / acetonitrile / 20 °C / Inert atmosphere

10.1: dmap; triethylamine / dichloromethane / 24 h / 30 °C / Inert atmosphere

With chromium dichloride; dmap; Schwartz's reagent; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; oxalyl dichloride; (R)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methanesulfonamide; indium iodide; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; toluene; acetonitrile; benzene; 1.1: Marshall reaction / 5.1: Swarts reaction / 9.1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1002/anie.201106762