N-[O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl]-4-octadecyloxybenzamide

Base Information

Chemical Name:N-[O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl]-4-octadecyloxybenzamide
CAS No.:503306-44-3
Molecular Formula:C₆₁H₇₃NO₁₂
Molecular Weight:1012.25
Hs Code.:

Synonyms:N-[O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl]-4-octadecyloxybenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl]-4-octadecyloxybenzamide

Chemical Property:

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Technology Process of N-[O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl]-4-octadecyloxybenzamide

There total 4 articles about N-[O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl]-4-octadecyloxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 183901-63-5
2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

: 503306-37-4
N-(2-hydroxyethyl)-4-octadecyloxybenzamide

: 503306-44-3
N-[O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl]-4-octadecyloxybenzamide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/S0968-0896(02)00266-3

Reference yield:

: 112-89-0
1-Bromooctadecane

: 503306-44-3
N-[O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl]-4-octadecyloxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃ / dimethylformamide / 65 °C

1.2: 88 percent / dimethylformamide / 30 h / 65 °C

2.1: 81 percent / dimethylformamide / 64 h / 110 °C

3.1: TMSOTf / CH₂Cl₂ / 0 - 20 °C

With trimethylsilyl trifluoromethanesulfonate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(02)00266-3

Reference yield:

: 360560-29-8
octadecyl 4-octadecyloxybenzoate

: 503306-44-3
N-[O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)oxyethyl]-4-octadecyloxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / dimethylformamide / 64 h / 110 °C

2: TMSOTf / CH₂Cl₂ / 0 - 20 °C

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(02)00266-3