(E)-methyl N--2-aminocinnamate

Base Information

• Chemical Name: (E)-methyl N--2-aminocinnamate
• CAS No.: 146668-22-6
• Molecular Formula: C₁₃H₁₅NO₂S₂
• Molecular Weight: 281.4

Synonyms:(E)-methyl N--2-aminocinnamate

Chemical Property of (E)-methyl N--2-aminocinnamate

Chemical Property:

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Technology Process of (E)-methyl N--2-aminocinnamate

There total 5 articles about (E)-methyl N--2-aminocinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

methyl threo-N-phenylserinate → (E)-methyl N--2-aminocinnamate (146668-22-6)

Guidance literature:

With copper(l) chloride; diisopropyl-carbodiimide; In dichloromethane; for 20h;

DOI:10.1016/S0040-4020(01)80317-3

Reference yield:

methyl threo-3-trimethylsilyloxy-2-N-amino-3-phenylpropanoate → (E)-methyl N--2-aminocinnamate (146668-22-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / Dowex-50W₈X, H₂₀ / methanol / 2 h / Ambient temperature

2: 60 percent / 1,2-diisopropylcarbodiimide, CuCl / CH₂Cl₂ / 20 h

With Dowex-50W₈X; water; copper(l) chloride; diisopropyl-carbodiimide; In methanol; dichloromethane;

DOI:10.1016/S0040-4020(01)80317-3

Reference yield:

methyl threo-3-trimethylsilyloxy-2-methylthiocarbamoyl-3-phenylpropanoate → (E)-methyl N--2-aminocinnamate (146668-22-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / K₂CO₃ / acetone / 1 h / Heating

2: 75 percent / Dowex-50W₈X, H₂₀ / methanol / 2 h / Ambient temperature

3: 60 percent / 1,2-diisopropylcarbodiimide, CuCl / CH₂Cl₂ / 20 h

With Dowex-50W₈X; water; potassium carbonate; copper(l) chloride; diisopropyl-carbodiimide; In methanol; dichloromethane; acetone;

DOI:10.1016/S0040-4020(01)80317-3

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