4-methylphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:4-methylphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside
CAS No.:77667-61-9
Molecular Formula:C₄₁H₄₂O₆
Molecular Weight:630.781
Hs Code.:

Synonyms:4-methylphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

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Chemical Property of 4-methylphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

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Technology Process of 4-methylphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

There total 4 articles about 4-methylphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 194088-19-2
(2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-2-(benzyloxymethyl)-6-(prop-2-ynyloxy)tetrahydro-2H-pyran

: 106-44-5
p-cresol

: 77667-61-9
4-methylphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Guidance literature:: With FeCl₃/C; In acetonitrile; at 60 ℃; for 6h; stereoselective reaction; Inert atmosphere; Green chemistry;
DOI:10.1055/s-0037-1611801

Reference yield: 78.0%

: 106-44-5
p-cresol

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 77667-61-9
4-methylphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Guidance literature:: With pyrylium tetrafluoroborate; In diethyl ether; at 23 ℃; for 2h; diastereoselective reaction; Sealed tube;
DOI:10.1002/anie.202115394

Reference yield:

: 17902-32-8
trimethyl(4-methylphenoxy)silane

: 89825-08-1
2,3,4,6-tetra-O-benzyl-1-O-trimethylsilyl-α,β-D-glucopyranose

: 77667-61-9
4-methylphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

: 74808-11-0
p-methylphenyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Guidance literature:: trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 24h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)85681-6