3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-1,1-dioxo-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole

Base Information

Chemical Name:3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-1,1-dioxo-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole
CAS No.:1285576-39-7
Molecular Formula:C₁₈H₁₀F₆N₂O₄S
Molecular Weight:464.345
Hs Code.:

Synonyms:3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-1,1-dioxo-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole

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Chemical Property of 3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-1,1-dioxo-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole

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Technology Process of 3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-1,1-dioxo-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole

There total 12 articles about 3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-1,1-dioxo-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1285576-36-4
3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole

: 1285576-39-7
3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-1,1-dioxo-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 0 ℃; for 40h;

Reference yield:

: 1285573-63-8
3-formyl-4-methoxy-5-trifluoromethylbenzoic acid

: 1285576-39-7
3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-1,1-dioxo-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole

Guidance literature:: Multi-step reaction with 4 steps

1: formic acid; hydroxylamine hydrochloride / 19 h / Reflux

2: thionyl chloride / N,N-dimethyl-formamide / toluene / 16 h / 60 °C

3: triethylamine / dichloromethane / 1.5 h / 20 °C

4: 3-chloro-benzenecarboperoxoic acid / chloroform / 40 h / 0 °C

With formic acid; thionyl chloride; hydroxylamine hydrochloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; N,N-dimethyl-formamide; In dichloromethane; chloroform; toluene;

Reference yield:

: 1285573-58-1
5-bromo-1-diethoxymethyl-2-methoxy-3-trifluoromethylbenzene

: 1285576-39-7
3-(3-cyano-4-methoxy-5-trifluoromethylbenzoyl)-1,1-dioxo-5-trifluoromethyl-2,3-dihydro-1,3-benzothiazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium / tetrahydrofuran / 1.5 h / 20 °C

1.2: 1 h / 0 °C

1.3: 16 h / 20 °C

2.1: formic acid; hydroxylamine hydrochloride / 19 h / Reflux

3.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 16 h / 60 °C

4.1: triethylamine / dichloromethane / 1.5 h / 20 °C

5.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 40 h / 0 °C

With formic acid; thionyl chloride; hydroxylamine hydrochloride; magnesium; triethylamine; 3-chloro-benzenecarboperoxoic acid; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; chloroform; toluene;