N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester

Base Information

Chemical Name:N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester
CAS No.:129575-02-6
Molecular Formula:C₃₃H₅₆N₄O₈Si
Molecular Weight:664.915
Hs Code.:

N-<trans-3-<4-<2-amino-1-<(1,1-dimethylethyl)dimethylsilyloxy>oxy>ethyl>-phenoxy>-1-<N-(1,1-dimethylethoxycarbonyl)glycyl>-L-prolyl-L-isoleucine methyl ester

Synonyms:N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester

Suppliers and Price of N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester

There total 4 articles about N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.8%

: 129575-01-5
N-<1-glycyl>-trans-3-<4-(1,1-dimethylethyl)dimethylsilyloxy>-2-(nitroethyl)phenoxy-L-prolyl-L-isoleucine methyl ester

: 129575-02-6
N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 7.5h; Ambient temperature;

Reference yield:

: 123043-38-9,123043-39-0
N-trans-3-(4-cyanophenoxy)-1-glycyl>-L-prolyl-L-isoleucine methyl ester

: 129575-02-6
N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 76.4 percent / Raney Ni, NaH₂PO₂*H₂O, buffer 2:1:1 pyridine: acetic acid: water / 4 h / 55 - 60 °C

2: 93.6 percent / sodium methoxide / 3.5 h / 0 °C

3: 94.8 percent / imidazole / dimethylformamide / 1.) 0 deg C, 30 min, 2.) RT, 9.5 h

4: 87.8 percent / ammonium formate / Pd/C / methanol / 7.5 h / Ambient temperature

With 1H-imidazole; sodium hypophosphite; buffer 2:1:1 pyridine: acetic acid: water; sodium methylate; ammonium formate; nickel; isobutyric Acid; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 129574-99-8
N-<1-glycyl>-trans-3-<4-(formylphenoxy)-L-prolyl>-L-isoleucine methyl ester

: 129575-02-6
N-oxy>ethyl>-phenoxy>-1--L-prolyl-L-isoleucine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93.6 percent / sodium methoxide / 3.5 h / 0 °C

2: 94.8 percent / imidazole / dimethylformamide / 1.) 0 deg C, 30 min, 2.) RT, 9.5 h

3: 87.8 percent / ammonium formate / Pd/C / methanol / 7.5 h / Ambient temperature

With 1H-imidazole; sodium methylate; ammonium formate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;