tert-butyl (6-((2,6-dichlorobenzyl)oxy)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate

Base Information

Chemical Name:tert-butyl (6-((2,6-dichlorobenzyl)oxy)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate
CAS No.:1361519-55-2
Molecular Formula:C₂₀H₂₀Cl₂N₂O₅
Molecular Weight:439.295
Hs Code.:

Synonyms:tert-butyl (6-((2,6-dichlorobenzyl)oxy)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate

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Chemical Property of tert-butyl (6-((2,6-dichlorobenzyl)oxy)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate

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Technology Process of tert-butyl (6-((2,6-dichlorobenzyl)oxy)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate

There total 6 articles about tert-butyl (6-((2,6-dichlorobenzyl)oxy)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1361519-54-1
tert-butyl (6-hydroxy-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate

: 20443-98-5
2,6-Dichlorobenzyl bromide

: 1361519-55-2
tert-butyl (6-((2,6-dichlorobenzyl)oxy)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃;
DOI:10.1002/chem.201102732

Reference yield:

: 1361519-52-9
8-amino-6-methoxy-2H-1,4-benzoxazin-3(4H)-one

: 1361519-55-2
tert-butyl (6-((2,6-dichlorobenzyl)oxy)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: water; hydrogen bromide; acetic acid / Reflux

2: triethylamine / ethanol; water / 72 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 20 °C

With water; hydrogen bromide; potassium carbonate; acetic acid; triethylamine; In ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201102732

Reference yield:

: 4-methoxy-2,6-diaminophenol dihydrochloride

: 1361519-55-2
tert-butyl (6-((2,6-dichlorobenzyl)oxy)-3-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazin-8-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / water; acetonitrile / 0.42 h / Inert atmosphere; Reflux

2: water; hydrogen bromide; acetic acid / Reflux

3: triethylamine / ethanol; water / 72 h / 20 °C

4: potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 20 °C

With water; hydrogen bromide; potassium carbonate; acetic acid; triethylamine; In ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201102732