C₃₄H₃₇BrO

Base Information

• Chemical Name: C₃₄H₃₇BrO
• CAS No.: 1422556-52-2
• Molecular Formula: C₃₄H₃₇BrO
• Molecular Weight: 541.571
• Mol file: 1422556-52-2.mol

Synonyms:C₃₄H₃₇BrO

Chemical Property of C₃₄H₃₇BrO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₇BrO

There total 5 articles about C₃₄H₃₇BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

9-bromo-10-ethynylanthracene + 1-(dodecyloxy)-4-iodobenzene (116223-59-7) → C34H37BrO (1422556-52-2)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; at 75 ℃; Inert atmosphere;

DOI:10.1021/la304920j

Reference yield:

1-dodecylbromide (143-15-7) → C34H37BrO (1422556-52-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 70 °C

2: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 75 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/la304920j

Reference yield:

9,10-Dibromoanthracene (523-27-3) → C34H37BrO (1422556-52-2)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 75 °C / Inert atmosphere

2: sodium hydride / toluene / 0.33 h / 80 °C

3: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 75 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; triethylamine; In tetrahydrofuran; toluene;

DOI:10.1021/la304920j

upstream raw materials:

1-(dodecyloxy)-4-iodobenzene

p-Iodophenol

1-dodecylbromide

9-bromo-10-(3-hydroxy-3-methylbutyn-1-yl)anthracene

Downstream raw materials:

C₅₂H₆₄N₂O₃

C₃₄H₃₇IO