4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside

Base Information

Chemical Name:4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside
CAS No.:1609690-82-5
Molecular Formula:C₂₇H₂₇ClO₉
Molecular Weight:530.959
Hs Code.:

Synonyms:4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside

Suppliers and Price of 4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside

There total 4 articles about 4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 16741-27-8
2,3,4-tri-O-acetyl-α-L-fucopyranosyl bromide

: 1609690-73-4
5-chloro-2-(4-hydroxyphenyl)-3-methylbenzofuran

: 1609690-82-5
4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In chloroform; water; at 20 ℃; for 24h;
DOI:10.1016/j.carres.2014.03.006

Reference yield:

: 695-96-5
2-bromo-4-chlorophenol

: 1609690-82-5
4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium diacetate; racemic-2-(di-tert-butylphosphino)-1,1′-binaphthyl; sodium t-butanolate / toluene / 1 h / 100 °C / Microwave irradiation

1.2: 20 °C

2.1: sodium thioethylate / N,N-dimethyl-formamide / 4 h / 145 °C

3.1: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / chloroform; water / 24 h / 20 °C

With racemic-2-(di-tert-butylphosphino)-1,1′-binaphthyl; tetra(n-butyl)ammonium hydrogensulfate; palladium diacetate; potassium carbonate; sodium t-butanolate; sodium thioethylate; In chloroform; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.carres.2014.03.006

Reference yield:

: 1056899-49-0
5-chloro-2-(4-methoxyphenyl)-3-methylbenzofuran

: 1609690-82-5
4-[5-chloro-3-methylbenzofuran-2-yl]phenyl tri-O-acetyl-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium thioethylate / N,N-dimethyl-formamide / 4 h / 145 °C

2: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / chloroform; water / 24 h / 20 °C

With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; sodium thioethylate; In chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2014.03.006