methyl (2E)-8-benzyloxy-4-methyl-3-<(diethoxy)phosphoryloxy>-2-octenoate

Base Information

Chemical Name:methyl (2E)-8-benzyloxy-4-methyl-3-<(diethoxy)phosphoryloxy>-2-octenoate
CAS No.:129512-08-9
Molecular Formula:C₂₁H₃₃O₇P
Molecular Weight:428.463
Hs Code.:

Synonyms:methyl (2E)-8-benzyloxy-4-methyl-3-<(diethoxy)phosphoryloxy>-2-octenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2E)-8-benzyloxy-4-methyl-3-<(diethoxy)phosphoryloxy>-2-octenoate

Chemical Property:

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Technology Process of methyl (2E)-8-benzyloxy-4-methyl-3-<(diethoxy)phosphoryloxy>-2-octenoate

There total 3 articles about methyl (2E)-8-benzyloxy-4-methyl-3-<(diethoxy)phosphoryloxy>-2-octenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30414-53-0
methyl propanoyl acetate

: 129512-08-9
methyl (2E)-8-benzyloxy-4-methyl-3-<(diethoxy)phosphoryloxy>-2-octenoate

Guidance literature:: Multi-step reaction with 2 steps

2: 1) NEt₃, HMPT, 2) 4-dimethylaminopyridine / 1) 0 deg C, 1h, 2) RT, 6h

With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; triethylamine;
DOI:10.1055/s-1990-26881

Reference yield:

: 60789-54-0
4-bromobutyl benzyl ether

: 129512-08-9
methyl (2E)-8-benzyloxy-4-methyl-3-<(diethoxy)phosphoryloxy>-2-octenoate

Guidance literature:: Multi-step reaction with 2 steps

2: 1) NEt₃, HMPT, 2) 4-dimethylaminopyridine / 1) 0 deg C, 1h, 2) RT, 6h

With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; triethylamine;
DOI:10.1055/s-1990-26881

Reference yield:

: 129512-09-0
methyl 8-benzyloxy-4-methyl-3-oxooctanoate

: 814-49-3
diethyl chlorophosphate

: 129512-08-9
methyl (2E)-8-benzyloxy-4-methyl-3-<(diethoxy)phosphoryloxy>-2-octenoate

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; triethylamine; Yield given. Multistep reaction; 1) 0 deg C, 1h, 2) RT, 6h;
DOI:10.1055/s-1990-26881