methyl (3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-yl) carbonate

Base Information

Chemical Name:methyl (3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-yl) carbonate
CAS No.:1393090-06-6
Molecular Formula:C₂₃H₁₆O₃S
Molecular Weight:372.444
Hs Code.:

Synonyms:methyl (3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-yl) carbonate

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Chemical Property of methyl (3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-yl) carbonate

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Technology Process of methyl (3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-yl) carbonate

There total 2 articles about methyl (3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-yl) carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1393090-37-3
3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-ol

: 79-22-1
methyl chloroformate

: 1393090-06-6
methyl (3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-yl) carbonate

Guidance literature:: 3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-ol; With dmap; triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;

methyl chloroformate; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201201799

Reference yield: 86.0%

: 2-(thiophen-2-ylethynyl)-benzaldehyde

: 79-22-1
methyl chloroformate

: 536-74-3
phenylacetylene

: 1393090-06-6
methyl (3-phenyl-1-(2-(thiophen-2-ylethynyl)phenyl)prop-2-yn-1-yl) carbonate

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

2-(thiophen-2-ylethynyl)-benzaldehyde; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

methyl chloroformate; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201601074