ALLYLPHOSPHONIC ACID

Base Information

• Chemical Name: ALLYLPHOSPHONIC ACID
• CAS No.: 6833-67-6
• Molecular Formula: C3H7 O3 P
• Molecular Weight: 122.059641
• Hs Code.: 2931900090
• Mol file: 6833-67-6.mol

Synonyms:Phosphonicacid, 2-propenyl- (9CI); Phosphonic acid, allyl- (7CI,8CI);2-Propene-1-phosphonic acid; Allylphosphonic acid

Chemical Property of ALLYLPHOSPHONIC ACID

Chemical Property:

• Melting Point: 47-50 °C
• PSA: 67.34000
• LogP: 0.35010

Purity/Quality:

99% ^*data from raw suppliers

ALLYLPHOSPHONIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 22-34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ALLYLPHOSPHONIC ACID

There total 5 articles about ALLYLPHOSPHONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Diethyl allylphosphonate (1067-87-4) → allylphosphonic acid (6833-67-6)

Guidance literature:

Diethyl allylphosphonate; With trimethylsilyl bromide; In dichloromethane; for 24h; Inert atmosphere;

In methanol; for 24h; Inert atmosphere;

DOI:10.1002/anie.201005173

Reference yield: 89.0%

allylphosphonic acid dimethyl ester (757-54-0) → allylphosphonic acid (6833-67-6)

Guidance literature:

With trifluorormethanesulfonic acid; In water; at 140 ℃; for 24h; Sealed tube; Schlenk technique;

DOI:10.1021/acs.joc.0c00550

Reference yield: 50.0%

→ allylphosphonic acid (6833-67-6)

Guidance literature:

upstream raw materials:

bis(4-methoxyphenyl) allylphosphonate

allylphosphonic acid dimethyl ester

Diethyl allylphosphonate

Downstream raw materials:

propene