methyl O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:methyl O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside
CAS No.:149827-74-7
Molecular Formula:C₃₆H₄₃NO₁₀
Molecular Weight:649.738
Hs Code.:

Synonyms:methyl O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of methyl O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

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Technology Process of methyl O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

There total 2 articles about methyl O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl O-(2-azido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

: 149827-74-7
methyl O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NiCl₂, H₃BO₃, NaBH₄ / ethanol / 1 h / 25 °C

2: ethanol / 0 °C

With sodium tetrahydroborate; boric acid; nickel dichloride; In ethanol;
DOI:10.1016/0008-6215(94)84079-2

Reference yield:

: 108-24-7
acetic anhydride

: (2R,4aR,6R,7R,8R,8aS)-7-Amino-6-((2R,3R,4R,5S,6S)-3,5-bis-benzyloxy-2-methoxy-6-methyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

: 149827-74-7
methyl O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: In ethanol; at 0 ℃; Yield given;
DOI:10.1016/0008-6215(94)84079-2

Reference yield: 87.0%

: 149827-74-7
methyl O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

: 149827-85-0
methyl 3,4,6-tri-O-benzyl-2-O-(4-methoxybenzyl)-1-thio-β-D-galactopyranoside

: 149827-75-8
methyl O-<3,4,6-tri-O-benzyl-2-O-(4-methoxybenzyl)-α-D-galactopyranosyl>-(1<*>3)-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1<*>3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; 4 A molecular sieve; methyl trifluoromethanesulfonate; In diethyl ether; at 25 ℃; for 60h;
DOI:10.1016/0008-6215(94)84079-2