[3-chloro-4-(fluorosulfonyl)benzyl](triphenyl)phosphonium

Base Information

• Chemical Name: [3-chloro-4-(fluorosulfonyl)benzyl](triphenyl)phosphonium
• CAS No.: 31362-36-4
• Molecular Formula: Br*C₂₅H₂₀ClFO₂PS
• Molecular Weight: 549.828
• Mol file: 31362-36-4.mol

Synonyms:Phosphonium,[3-chloro-4-(fluorosulfonyl)benzyl]triphenyl-, bromide (8CI); NSC 210269

Chemical Property of [3-chloro-4-(fluorosulfonyl)benzyl](triphenyl)phosphonium

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [3-chloro-4-(fluorosulfonyl)benzyl](triphenyl)phosphonium

There total 1 articles about [3-chloro-4-(fluorosulfonyl)benzyl](triphenyl)phosphonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenylphosphine (603-35-0) + 4-Bromomethyl-2-chloro-benzenesulfonyl fluoride → 3-Chlor-4-fluorsulfonylbenzyltriphenylphosphonium (31362-36-4)

Guidance literature:

In benzene; Heating;

DOI:10.1021/jm00300a030

Reference yield:

3-nitrocinnamaldehyde (1504-76-3) + 3-Chlor-4-fluorsulfonylbenzyltriphenylphosphonium (31362-36-4) → 2-Chloro-4-[(1E,3E)-4-(3-nitro-phenyl)-buta-1,3-dienyl]-benzenesulfonyl fluoride (31368-36-2)

Guidance literature:

DOI:10.1021/jm00300a030

Reference yield:

(E)-3-(2-Chloro-4-nitro-phenyl)-propenal (24893-01-4) + 3-Chlor-4-fluorsulfonylbenzyltriphenylphosphonium (31362-36-4) → 2-Chloro-4-[(1E,3E)-4-(2-chloro-4-nitro-phenyl)-buta-1,3-dienyl]-benzenesulfonyl fluoride (31368-26-0)

Guidance literature:

DOI:10.1021/jm00300a030

upstream raw materials:

triphenylphosphine

Downstream raw materials:

2-Chloro-4-[(1E,3E)-4-(3-nitro-phenyl)-buta-1,3-dienyl]-benzenesulfonyl fluoride

2-Chloro-4-[(E)-2-(2-chloro-4-nitro-phenyl)-vinyl]-benzenesulfonyl fluoride

2-Chloro-4-[(1E,3E)-4-(2-chloro-4-nitro-phenyl)-buta-1,3-dienyl]-benzenesulfonyl fluoride

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