5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide

Base Information

• Chemical Name: 5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide
• CAS No.: 104947-43-5
• Molecular Formula: C₃₆H₄₆N₂O₄S₂
• Molecular Weight: 634.904

Synonyms:5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide

Chemical Property of 5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide

There total 10 articles about 5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-bis(4-methoxyphenyl)butanone (4390-94-7) → 5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide (104947-43-5)

Guidance literature:

Multi-step reaction with 9 steps

1: TsOH

2: 0 °C

3: 1.) BH₃, 2.) NaOH, H₂O₂ / 1.) THF

4: Ph₃P, diisopropyl azodicarboxylate

5: LiAlH₄

6: KH

7: LiAlH₄

8: Et₃N

9: TsOH

With sodium hydroxide; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; borane; dihydrogen peroxide; potassium hydride; toluene-4-sulfonic acid; triethylamine; triphenylphosphine;

DOI:10.1021/jm00384a026

Reference yield:

5-Dimethylamino-naphthalene-1-sulfonic acid (7-{(2S,3R)-2,3-bis-[4-(1-ethoxy-ethoxy)-phenyl]-pentylsulfanyl}-heptyl)-amide (104947-42-4) → 5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide (104947-43-5)

Guidance literature:

With toluene-4-sulfonic acid;

DOI:10.1021/jm00384a026

Reference yield:

7-bromo-heptanonitrile (20965-27-9) → 5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide (104947-43-5)

Guidance literature:

Multi-step reaction with 4 steps

1: KH

2: LiAlH₄

3: Et₃N

4: TsOH

With lithium aluminium tetrahydride; potassium hydride; toluene-4-sulfonic acid; triethylamine;

DOI:10.1021/jm00384a026

upstream raw materials:

5-Dimethylamino-naphthalene-1-sulfonic acid (7-{(2S,3R)-2,3-bis-[4-(1-ethoxy-ethoxy)-phenyl]-pentylsulfanyl}-heptyl)-amide

7-bromo-heptanonitrile

1,2-bis(4-methoxyphenyl)butanone

C₂₅H₃₄O₄

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 104947-43-5 5-Dimethylamino-naphthalene-1-sulfonic acid {7-[(2S,3R)-2,3-bis-(4-hydroxy-phenyl)-pentylsulfanyl]-heptyl}-amide

Send

Send

Metric Ton KG G Pound L ML

Send

Send