4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane

Base Information

Chemical Name:4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane
CAS No.:1160930-63-1
Molecular Formula:C₄₄H₅₄B₂O₄S₄Si₂
Molecular Weight:852.967
Hs Code.:

Synonyms:4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane

Suppliers and Price of 4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane

There total 3 articles about 4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 13321-36-3
di-tert-butylsilanediol

: 1160930-73-3
4-(2,2'-bithiophen-5-yl)phenylboronic acid

: 1160930-63-1
4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane

Guidance literature:: In toluene; for 30h; Inert atmosphere; Reflux;

Reference yield:

: 1160930-69-7
5-(4-bromophenyl)-[2,2']bithiophene

: 1160930-63-1
4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane

Guidance literature:: Multi-step reaction with 3 steps

1: PdCl₂((C₆H₅)2PC₅H₄)2Fe; CH₃COOK / 1,4-dioxane

2: HCl / tetrahydrofuran; hydrogenchloride

3: toluene

With PdCl₂((C₆H₅)2PC₅H₄)2Fe; CH₃COOK; HCl; In tetrahydrofuran; 1,4-dioxane; hydrogenchloride; toluene;

Reference yield:

: 1160930-70-0
2-(4-(2,2'-bithiophen-5-yl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1160930-63-1
4,8-bis(4-(2,2'-bithiophen-5-yl)phenyl)-2,2,6,6-tetra-tert-butyl-1,3,5,7,2,6,4,8-tetraoxadisiladiborocane

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / tetrahydrofuran; hydrogenchloride

2: toluene

With HCl; In tetrahydrofuran; hydrogenchloride; toluene;