3-{4-[4-(2-carboxyvinyl)-2-trifluoromethyl-phenylsulfanyl]-3-trifluoromethyl-phenyl}-acrylic acid dimethyl ester

Base Information

Chemical Name:3-{4-[4-(2-carboxyvinyl)-2-trifluoromethyl-phenylsulfanyl]-3-trifluoromethyl-phenyl}-acrylic acid dimethyl ester
CAS No.:719293-98-8
Molecular Formula:C₂₂H₁₆F₆O₄S
Molecular Weight:490.423
Hs Code.:

Synonyms:3-{4-[4-(2-carboxyvinyl)-2-trifluoromethyl-phenylsulfanyl]-3-trifluoromethyl-phenyl}-acrylic acid dimethyl ester

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Chemical Property of 3-{4-[4-(2-carboxyvinyl)-2-trifluoromethyl-phenylsulfanyl]-3-trifluoromethyl-phenyl}-acrylic acid dimethyl ester

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Technology Process of 3-{4-[4-(2-carboxyvinyl)-2-trifluoromethyl-phenylsulfanyl]-3-trifluoromethyl-phenyl}-acrylic acid dimethyl ester

There total 4 articles about 3-{4-[4-(2-carboxyvinyl)-2-trifluoromethyl-phenylsulfanyl]-3-trifluoromethyl-phenyl}-acrylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 719293-97-7
4,4'-diiodo-2,2'-bis(trifluoromethyl)diphenylsulfide

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 719293-98-8
3-{4-[4-(2-carboxyvinyl)-2-trifluoromethyl-phenylsulfanyl]-3-trifluoromethyl-phenyl}-acrylic acid dimethyl ester

Guidance literature:: With triethylamine; palladium diacetate; triphenylphosphine; In DMF (N,N-dimethyl-formamide); at 110 ℃; for 9h; Heating / reflux;

Reference yield:

: 400-77-1
4-nitro-2-trifluoromethylthiophenol

: 719293-98-8
3-{4-[4-(2-carboxyvinyl)-2-trifluoromethyl-phenylsulfanyl]-3-trifluoromethyl-phenyl}-acrylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine / iron(III) chloride / ethanol / 32 h / Heating / reflux; Activated charcoal

2: hydrogenchloride; sodium nitrite / water / 0 °C

3: triethylamine / palladium diacetate; triphenylphosphine / DMF (N,N-dimethyl-formamide) / 9 h / 110 °C / Heating / reflux

With hydrogenchloride; triethylamine; hydrazine; sodium nitrite; iron(III) chloride; palladium diacetate; triphenylphosphine; In DMF (N,N-dimethyl-formamide); ethanol; water;

Reference yield:

: 777-37-7
4-chloro-3-(trifluoromethyl)nitrobenzene

: 719293-98-8
3-{4-[4-(2-carboxyvinyl)-2-trifluoromethyl-phenylsulfanyl]-3-trifluoromethyl-phenyl}-acrylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium sulfide / water / 6 h / 100 °C / Heating / reflux

2: hydrazine / iron(III) chloride / ethanol / 32 h / Heating / reflux; Activated charcoal

3: hydrogenchloride; sodium nitrite / water / 0 °C

4: triethylamine / palladium diacetate; triphenylphosphine / DMF (N,N-dimethyl-formamide) / 9 h / 110 °C / Heating / reflux

With hydrogenchloride; sodium sulfide; triethylamine; hydrazine; sodium nitrite; iron(III) chloride; palladium diacetate; triphenylphosphine; In DMF (N,N-dimethyl-formamide); ethanol; water;