2-(3-chloropropyl)-2-carboethoxycyclohexanone

Base Information

Chemical Name:2-(3-chloropropyl)-2-carboethoxycyclohexanone
CAS No.:360568-56-5
Molecular Formula:C₁₂H₁₉ClO₃
Molecular Weight:246.734
Hs Code.:

Synonyms:2-(3-chloropropyl)-2-carboethoxycyclohexanone

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Chemical Property of 2-(3-chloropropyl)-2-carboethoxycyclohexanone

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Technology Process of 2-(3-chloropropyl)-2-carboethoxycyclohexanone

There total 1 articles about 2-(3-chloropropyl)-2-carboethoxycyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 6940-76-7
1-iodo-3-chloro-propane

: 1655-07-8
ethyl 2-oxocyclohexane carboxylate

: 360568-56-5
2-(3-chloropropyl)-2-carboethoxycyclohexanone

Guidance literature:: ethyl 2-oxocyclohexane carboxylate; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

1-iodo-3-chloro-propane; at 23 ℃; for 48h;
DOI:10.1021/acs.joc.1c01650

Reference yield: 83.0%

: 360568-56-5
2-(3-chloropropyl)-2-carboethoxycyclohexanone

: ethyl 1-(3-azidopropyl)-2-oxocyclohexanecarboxylate

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.1021/acs.joc.1c01650

Reference yield: 68.0%

: 360568-56-5
2-(3-chloropropyl)-2-carboethoxycyclohexanone

: 137125-32-7
ethyl 5-oxooctahydro-1H-pyrrolo[1,2-a]azepine-9a-carboxylate

: ethyl 1-(3-azidopropyl)-2-oxocyclohexanecarboxylate

Guidance literature:: 2-(3-chloropropyl)-2-carboethoxycyclohexanone; With tetrabutylammoniun azide; In acetonitrile; Inert atmosphere; Microwave irradiation;

With trifluoroacetic acid; In acetonitrile; under 2068.65 Torr; Microwave irradiation; Inert atmosphere;
DOI:10.1002/chem.201100768