(S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid

Base Information

Chemical Name:(S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid
CAS No.:1314531-79-7
Molecular Formula:C₁₈H₁₈N₂O₅
Molecular Weight:342.351
Hs Code.:

Synonyms:(S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid

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Chemical Property of (S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid

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Technology Process of (S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid

There total 6 articles about (S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1314531-71-9
(S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid methyl ester

: 1314531-79-7
(S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid

Guidance literature:: With water; lithium hydroxide; In methanol; at 0 - 20 ℃; for 5h;
DOI:10.1002/cmdc.201100093

Reference yield:

: 1314531-61-7
(2-oxo-1,2-dihydropyridin-3-yl)carbamic acid allyl ester

: 1314531-79-7
(S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: water; lithium hydroxide / methanol / 5 h / 0 - 20 °C

With water; sodium hydride; lithium hydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201100093

Reference yield:

: 173327-33-8
(R)-2-methanesulfonyloxy-3-phenylpropionic acid methyl ester

: 1314531-79-7
(S)-2-(3-allyloxycarbonylamino-2-oxo-2H-pyridin-1-yl)-3-phenylpropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

1.2: 12 h / 20 °C

2.1: lithium hydroxide / methanol; water / 5 h / 20 °C

With sodium hydride; lithium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.molstruc.2020.129633