3-tert-butoxycarbonylamino-3-(1H-tetrazol-5-yl)propionic acid benzyl ester

Base Information

Chemical Name:3-tert-butoxycarbonylamino-3-(1H-tetrazol-5-yl)propionic acid benzyl ester
CAS No.:1548864-83-0
Molecular Formula:C₁₆H₂₁N₅O₄
Molecular Weight:347.374
Hs Code.:

Synonyms:3-tert-butoxycarbonylamino-3-(1H-tetrazol-5-yl)propionic acid benzyl ester

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Chemical Property of 3-tert-butoxycarbonylamino-3-(1H-tetrazol-5-yl)propionic acid benzyl ester

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Technology Process of 3-tert-butoxycarbonylamino-3-(1H-tetrazol-5-yl)propionic acid benzyl ester

There total 3 articles about 3-tert-butoxycarbonylamino-3-(1H-tetrazol-5-yl)propionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1548864-78-3
3-tert-butoxycarbonylamino-3-cyanopropionic acid benzyl ester

: 1548864-83-0
3-tert-butoxycarbonylamino-3-(1H-tetrazol-5-yl)propionic acid benzyl ester

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 110 ℃; for 3h; Inert atmosphere;

Reference yield:

: 147291-69-8,98482-77-0
4-(benzyloxy)-2-(tert-butoxycarbonylamino)-4-oxobutanoic acid

: 1548864-83-0
3-tert-butoxycarbonylamino-3-(1H-tetrazol-5-yl)propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.5 h / 0 °C

1.2: 1 h

2.1: pyridine; trifluoroacetic anhydride / 1,4-dioxane / 0.67 h / 0 - 15 °C

3.1: ammonium chloride; sodium azide / N,N-dimethyl-formamide / 3 h / 110 °C / Inert atmosphere

With pyridine; sodium azide; chloroformic acid ethyl ester; ammonium chloride; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 50715-49-6,87421-27-0
2-<(N-tert-butoxycarbonyl)amino>-3-benzyloxycarbonylbutanamide

: 1548864-83-0
3-tert-butoxycarbonylamino-3-(1H-tetrazol-5-yl)propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; trifluoroacetic anhydride / 1,4-dioxane / 0.67 h / 0 - 15 °C

2: ammonium chloride; sodium azide / N,N-dimethyl-formamide / 3 h / 110 °C / Inert atmosphere

With pyridine; sodium azide; ammonium chloride; trifluoroacetic anhydride; In 1,4-dioxane; N,N-dimethyl-formamide;