(3,4-dimethoxy-phenyl)-acetic acid-(β-hydroxy-3,4-dimethoxy-phenethylamide)

Base Information

Chemical Name:(3,4-dimethoxy-phenyl)-acetic acid-(β-hydroxy-3,4-dimethoxy-phenethylamide)
CAS No.:78004-24-7
Molecular Formula:C₂₀H₂₅NO₆
Molecular Weight:375.422
Hs Code.:

Synonyms:(3,4-dimethoxy-phenyl)-acetic acid-(β-hydroxy-3,4-dimethoxy-phenethylamide)

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Chemical Property of (3,4-dimethoxy-phenyl)-acetic acid-(β-hydroxy-3,4-dimethoxy-phenethylamide)

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Technology Process of (3,4-dimethoxy-phenyl)-acetic acid-(β-hydroxy-3,4-dimethoxy-phenethylamide)

There total 9 articles about (3,4-dimethoxy-phenyl)-acetic acid-(β-hydroxy-3,4-dimethoxy-phenethylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10313-60-7
3,4-dimethoxyphenylacetyl chloride

: 78004-24-7
(3,4-dimethoxy-phenyl)-acetic acid-(β-hydroxy-3,4-dimethoxy-phenethylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h

2: Et₃N, H₂₀ / CH₂Cl₂; tetrahydrofuran / 0.5 h

With water; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00331a038

Reference yield:

: 78004-17-8
5-(3,4-Dimethoxyphenyl)-2-oxazoline

: 78004-24-7
(3,4-dimethoxy-phenyl)-acetic acid-(β-hydroxy-3,4-dimethoxy-phenethylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h

2: Et₃N, H₂₀ / CH₂Cl₂; tetrahydrofuran / 0.5 h

With water; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00331a038

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 78004-24-7
(3,4-dimethoxy-phenyl)-acetic acid-(β-hydroxy-3,4-dimethoxy-phenethylamide)

Guidance literature:: Multi-step reaction with 3 steps

1: n-BuLi / 1.) THF, -78 deg C, 60 min; 2.) -60 deg C, 30 min

2: CH₂Cl₂ / 0.5 h

3: Et₃N, H₂₀ / CH₂Cl₂; tetrahydrofuran / 0.5 h

With n-butyllithium; water; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00331a038