C₁₃H₁₂ClN₃O₄S

Base Information

Chemical Name:C₁₃H₁₂ClN₃O₄S
CAS No.:1329991-74-3
Molecular Formula:C₁₃H₁₂ClN₃O₄S
Molecular Weight:341.775
Hs Code.:

C<sub>13</sub>H<sub>12</sub>ClN<sub>3</sub>O<sub>4</sub>S

Synonyms:C₁₃H₁₂ClN₃O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₂ClN₃O₄S

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Technology Process of C₁₃H₁₂ClN₃O₄S

There total 6 articles about C₁₃H₁₂ClN₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1329991-73-2
C₁₄H₁₄ClN₃O₆S₂

: 1329991-74-3
C₁₃H₁₂ClN₃O₄S

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 0.5h;

Reference yield:

: 39736-29-3
ethyl 4-amino-2-(methylthio)thiazol-5-carboxylate

: 1329991-74-3
C₁₃H₁₂ClN₃O₄S

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / dichloromethane / 1.25 h / 20 °C / Cooling with ice; Inert atmosphere

2: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / tetrahydrofuran / 3.25 h / 0 - 20 °C

3: potassium carbonate; ethanol / 1 h / Reflux

4: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Cooling with ice; Inert atmosphere

5: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.25 h / Reflux

6: sodium tetrahydroborate / ethanol / 0.5 h

With pyridine; sodium tetrahydroborate; ethanol; sodium hexamethyldisilazane; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; ethanol; dichloromethane; chloroform;

Reference yield:

: 1329991-65-2
C₉H₉F₃N₂O₃S₂

: 1329991-74-3
C₁₃H₁₂ClN₃O₄S

Guidance literature:: Multi-step reaction with 5 steps

1: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / tetrahydrofuran / 3.25 h / 0 - 20 °C

2: potassium carbonate; ethanol / 1 h / Reflux

3: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Cooling with ice; Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.25 h / Reflux

5: sodium tetrahydroborate / ethanol / 0.5 h

With sodium tetrahydroborate; ethanol; sodium hexamethyldisilazane; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; ethanol; chloroform;