Cyclohexyloxycarbonyloxymethyl (5R,6S)-3-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-7-oxo-6-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

Base Information

• Chemical Name: Cyclohexyloxycarbonyloxymethyl (5R,6S)-3-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-7-oxo-6-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate
• CAS No.: 859148-79-1
• Molecular Formula: C₂₉H₄₅N₃O₇Si
• Molecular Weight: 575.778

Synonyms:Cyclohexyloxycarbonyloxymethyl (5R,6S)-3-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-7-oxo-6-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

Chemical Property of Cyclohexyloxycarbonyloxymethyl (5R,6S)-3-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-7-oxo-6-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

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Technology Process of Cyclohexyloxycarbonyloxymethyl (5R,6S)-3-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-7-oxo-6-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

There total 3 articles about Cyclohexyloxycarbonyloxymethyl (5R,6S)-3-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-7-oxo-6-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Cyclohexyloxycarbonyloxymethyl {[(2R,3S)-3-(1-tert-butyldimethylsilyloxy)ethyl]-2-[2-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-2-oxoethyl]-4-oxo-1-azetidinyl} [tris(ethoxy)-λ5-phosphanylidene] acetate → Cyclohexyloxycarbonyloxymethyl (5R,6S)-3-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-7-oxo-6-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (859148-79-1)

Guidance literature:

With copper(l) iodide; In toluene; for 0.5h; Heating / reflux;

Reference yield:

cyclohexyloxycarbonyloxymethyl {(2R,3S)-3-[(1R)-1-(tert-butyldimethyl-silyloxy)ethyl]-2-[2-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-2-oxoethyl]-4-oxo-1-azetidinyl}(methyl(diphenyl)-λ5-phosphanylidene)acetate (859163-19-2) → Cyclohexyloxycarbonyloxymethyl (5R,6S)-3-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-7-oxo-6-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (859148-79-1)

Guidance literature:

In xylene; for 1.5h; Product distribution / selectivity; Heating / reflux;

Reference yield:

cyclohexyloxycarbonyloxymethyl {(2R,3S)-3-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-2-[2-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-2-oxoethyl]-4-oxo-1-azetidinyl}(triphenyl-λ5-phosphanylidene)acetate (859163-23-8) → Cyclohexyloxycarbonyloxymethyl (5R,6S)-3-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-7-oxo-6-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (859148-79-1)

Guidance literature:

In 1,3,5-trimethyl-benzene; for 1.16667h; Product distribution / selectivity; Heating / reflux;

upstream raw materials:

cyclohexyloxycarbonyloxymethyl {(2R,3S)-3-[(1R)-1-(tert-butyldimethyl-silyloxy)ethyl]-2-[2-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-2-oxoethyl]-4-oxo-1-azetidinyl}(methyl(diphenyl)-λ5-phosphanylidene)acetate

cyclohexyloxycarbonyloxymethyl {(2R,3S)-3-[(1R)-1-(tert-butyldimethylsilyloxy)ethyl]-2-[2-(1-ethyl-5-methyl-1H-pyrazol-3-yl)-2-oxoethyl]-4-oxo-1-azetidinyl}(triphenyl-λ5-phosphanylidene)acetate

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