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1,2-dihydroxy-3,5-dimethoxybenzene

Base Information Edit
  • Chemical Name:1,2-dihydroxy-3,5-dimethoxybenzene
  • CAS No.:21128-11-0
  • Molecular Formula:C8H10O4
  • Molecular Weight:170.165
  • Hs Code.:
  • Mol file:21128-11-0.mol
1,2-dihydroxy-3,5-dimethoxybenzene

Synonyms:1,2-dihydroxy-3,5-dimethoxybenzene

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Chemical Property of 1,2-dihydroxy-3,5-dimethoxybenzene Edit
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Technology Process of 1,2-dihydroxy-3,5-dimethoxybenzene

There total 10 articles about 1,2-dihydroxy-3,5-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogen; palladium dihydroxide; In methanol; at 20 ℃; for 18h;
DOI:10.1016/S0040-4039(00)00812-1
Guidance literature:
Multi-step reaction with 8 steps
2.1: 32 percent / K2CO3 / dimethylformamide / 72 h / 80 °C
3.1: 100 percent / K2CO3 / dimethylformamide / 3 h / 0 °C
4.1: 97 percent / DIBAH / CH2Cl2 / 3 h / -78 °C
5.1: 76 percent / PCC / CH2Cl2 / 2 h / 20 °C
6.1: 30 percent aq. hydrogen peroxide; phenylselenic acid / CH2Cl2 / 48 h / 20 °C
6.2: KOH / methanol / 0.5 h / 20 °C
7.1: KOH / dimethylsulfoxide / 3 h / 20 °C
8.1: 100 percent / hydrogen / 20 percent Pd(OH)2/C / methanol / 18 h / 20 °C
With potassium hydroxide; phenylselenate; hydrogen; dihydrogen peroxide; diisobutylaluminium hydride; potassium carbonate; pyridinium chlorochromate; palladium dihydroxide; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; 1.1: Esterification / 2.1: Condensation / 3.1: Methylation / 4.1: Reduction / 5.1: Oxidation / 6.1: Oxidation / 6.2: Hydrolysis / 7.1: Methylation / 8.1: Hydrogenolysis;
DOI:10.1016/S0040-4039(00)00812-1
Guidance literature:
Multi-step reaction with 7 steps
1.1: 32 percent / K2CO3 / dimethylformamide / 72 h / 80 °C
2.1: 100 percent / K2CO3 / dimethylformamide / 3 h / 0 °C
3.1: 97 percent / DIBAH / CH2Cl2 / 3 h / -78 °C
4.1: 76 percent / PCC / CH2Cl2 / 2 h / 20 °C
5.1: 30 percent aq. hydrogen peroxide; phenylselenic acid / CH2Cl2 / 48 h / 20 °C
5.2: KOH / methanol / 0.5 h / 20 °C
6.1: KOH / dimethylsulfoxide / 3 h / 20 °C
7.1: 100 percent / hydrogen / 20 percent Pd(OH)2/C / methanol / 18 h / 20 °C
With potassium hydroxide; phenylselenate; hydrogen; dihydrogen peroxide; diisobutylaluminium hydride; potassium carbonate; pyridinium chlorochromate; palladium dihydroxide; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; 1.1: Condensation / 2.1: Methylation / 3.1: Reduction / 4.1: Oxidation / 5.1: Oxidation / 5.2: Hydrolysis / 6.1: Methylation / 7.1: Hydrogenolysis;
DOI:10.1016/S0040-4039(00)00812-1
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