3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzyl alcohol

Base Information

Chemical Name:3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzyl alcohol
CAS No.:157826-54-5
Molecular Formula:C₂₀H₂₉ClO₃
Molecular Weight:352.901
Hs Code.:

Synonyms:3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzyl alcohol

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Chemical Property of 3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzyl alcohol

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Technology Process of 3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzyl alcohol

There total 6 articles about 3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105427-91-6
methyl 3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzoate

: 157826-54-5
3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1016/S0040-4039(00)84050-2

Reference yield:

: 58106-55-1
2,4-dihydroxy-3-bromo-6-methyl-benzoic acid methyl ester

: 157826-54-5
3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / SO₂Cl₂ / diethyl ether / 3.5 h / Ambient temperature

2: 1.41 g / K₂CO₃ / acetone / 2.5 h / Heating

3: 1.) BuLi, 2.) CuCC-C(OMe)Me₂ / 1.) hexane, THF, HMPA, -78 deg C, 30 min, 2.) 18 h -> room temperature

4: LiAlH₄ / diethyl ether / 0 °C

With lithium aluminium tetrahydride; n-butyllithium; sulfuryl dichloride; potassium carbonate; In diethyl ether; acetone;
DOI:10.1246/bcsj.67.1178

Reference yield:

: 105427-88-1
methyl 3-bromo-5-chloro-2,4-dihydroxy-6-methylbenzoate

: 157826-54-5
3-chloro-5-<(E)-3,7-dimethyl-2,6-octadienyl>-4,6-dimethoxy-2-methylbenzyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.41 g / K₂CO₃ / acetone / 2.5 h / Heating

2: 1.) BuLi, 2.) CuCC-C(OMe)Me₂ / 1.) hexane, THF, HMPA, -78 deg C, 30 min, 2.) 18 h -> room temperature

3: LiAlH₄ / diethyl ether / 0 °C

With lithium aluminium tetrahydride; n-butyllithium; potassium carbonate; In diethyl ether; acetone;
DOI:10.1246/bcsj.67.1178