3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole

Base Information

Chemical Name:3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole
CAS No.:1023279-05-1
Molecular Formula:C₃₂H₃₅Cl₃N₂O
Molecular Weight:570.002
Hs Code.:

Synonyms:3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole

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Chemical Property of 3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole

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Technology Process of 3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole

There total 9 articles about 3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1023279-03-9
3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1H-pyrazole

: 112-29-8
1-bromo dodecane

: 1023279-05-1
3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole

: 1023279-06-2
5-(2-benzyloxy-4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole

Guidance literature:: With potassium carbonate; In acetone; for 24h; Heating;
DOI:10.1007/s00706-007-0676-4

Reference yield:

: 6921-66-0
4-chloro-2-hydroxy acetophenone

: 1023279-05-1
3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / K₂CO₃; KI / acetone / 16 h / Heating

2: 21 percent / NaH / tetrahydrofuran / 3 h / Heating

3: 95 percent / hydrazine hydrate / methanol / 8 h / 20 °C

4: 47 percent / K₂CO₃ / acetone / 24 h / Heating

With sodium hydride; potassium carbonate; hydrazine hydrate; potassium iodide; In tetrahydrofuran; methanol; acetone; 2: Claisen condensation;
DOI:10.1007/s00706-007-0676-4

Reference yield:

: 76292-53-0
2'-benzyloxy-4'-chloroacetophenone

: 1023279-05-1
3-(2-benzyloxy-4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-decyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: 21 percent / NaH / tetrahydrofuran / 3 h / Heating

2: 95 percent / hydrazine hydrate / methanol / 8 h / 20 °C

3: 47 percent / K₂CO₃ / acetone / 24 h / Heating

With sodium hydride; potassium carbonate; hydrazine hydrate; In tetrahydrofuran; methanol; acetone; 1: Claisen condensation;
DOI:10.1007/s00706-007-0676-4