6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1-(1-phenylethyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide

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Chemical Name:6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1-(1-phenylethyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide
CAS No.:1396780-11-2
Molecular Formula:C₂₃H₂₂BrN₅O₂
Molecular Weight:480.364
Hs Code.:

Synonyms:6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1-(1-phenylethyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide

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Chemical Property of 6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1-(1-phenylethyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide

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Technology Process of 6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1-(1-phenylethyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide

There total 6 articles about 6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1-(1-phenylethyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.8%

: 1396779-74-0
6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide

: 585-71-7,38661-81-3
(1-bromoethyl)benzne

: 1396780-11-2
6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1-(1-phenylethyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; Reflux;

Reference yield:

: 3-cyano-2,4-dimethyl-2-hydroxypyridine

: 1396780-11-2
6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1-(1-phenylethyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; ammonia / Raney Ni / methanol

2: dimethyl sulfoxide / 0.25 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / Reflux

With ammonia; hydrogen; potassium carbonate; Raney Ni; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 6-bromo-1H-pyrazolo[3,4-b]pyridine-4-carboxylic acid ethyl ester

: 1396780-11-2
6-bromo-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-1-(1-phenylethyl)-1H-pyrazolo[3,4-b]pyridine-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; water / ethanol / 1 h / 60 °C

2: dimethyl sulfoxide / 0.25 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / Reflux

With water; potassium carbonate; sodium hydroxide; In ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;