(1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

Base Information

Chemical Name:(1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol
CAS No.:161596-05-0
Molecular Formula:C₂₈H₃₀O₄
Molecular Weight:430.544
Hs Code.:

Synonyms:(1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

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Chemical Property of (1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

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Technology Process of (1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

There total 33 articles about (1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 151693-61-7
(1S,2R,3R,4R)-1-O-benzoyl-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

: 161596-05-0
(1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 16h;
DOI:10.1016/j.tetlet.2007.03.031

Reference yield: 33.0%

: 163563-91-5
(4R,5R,6S)-5,6-Bis-benzyloxy-4-benzyloxymethyl-cyclohex-2-enone

: 161596-05-0
(1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride;
DOI:10.1021/jo00116a008

Reference yield:

: 163563-91-5
(4R,5R,6S)-5,6-Bis-benzyloxy-4-benzyloxymethyl-cyclohex-2-enone

: 161596-04-9
(1R,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

: 161596-05-0
(1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In tetrahydrofuran; ethanol; at -78 ℃; for 0.166667h; Title compound not separated from byproducts.;
DOI:10.1016/j.tetlet.2007.03.031