3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-chlorophenyl-4H-1,2,4-triazole

Base Information

• Chemical Name: 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-chlorophenyl-4H-1,2,4-triazole
• CAS No.: 1152333-40-8
• Molecular Formula: C₂₇H₂₇ClN₄O₉S
• Molecular Weight: 619.052

Synonyms:3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-chlorophenyl-4H-1,2,4-triazole

Chemical Property of 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-chlorophenyl-4H-1,2,4-triazole

Chemical Property:

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Technology Process of 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-chlorophenyl-4H-1,2,4-triazole

There total 1 articles about 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-chlorophenyl-4H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazole-3-thiol (74270-76-1) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → 3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-chlorophenyl-4H-1,2,4-triazole (1152333-40-8)

Guidance literature:

4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazole-3-thiol; With potassium hydroxide; In ethanol; at 20 ℃; for 0.5h;

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide; In ethanol; at 20 ℃; for 48h;

DOI:10.1002/jccs.200800124

Reference yield: 92.2%

3-S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-5-(4-pyridyl)-4-p-chlorophenyl-4H-1,2,4-triazole (1152333-40-8) → C19H19ClN4O5S (1152333-54-4)

Guidance literature:

With methanol; ammonia;

DOI:10.1002/jccs.200800124

upstream raw materials:

4-(4-chlorophenyl)-5-(pyridin-4-yl)-4H-1,2,4-triazole-3-thiol

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

Downstream raw materials:

C₁₉H₁₉ClN₄O₅S

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