5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-6-bromo-benzo[1,3]dioxole

Base Information

Chemical Name:5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-6-bromo-benzo[1,3]dioxole
CAS No.:153255-00-6
Molecular Formula:C₁₉H₁₇BrO₅S
Molecular Weight:437.311
Hs Code.:

Synonyms:5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-6-bromo-benzo[1,3]dioxole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-6-bromo-benzo[1,3]dioxole

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Technology Process of 5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-6-bromo-benzo[1,3]dioxole

There total 1 articles about 5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-6-bromo-benzo[1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5434-47-9
5-bromo-6-bromomethylbenzo[1,3]dioxole

: 3-hydroxycyclopent-1-enyl phenyl sulfone

: 153255-00-6
5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-6-bromo-benzo[1,3]dioxole

Guidance literature:: With potassium hydroxide; tetra-(n-butyl)ammonium iodide; In dichloromethane; at 25 ℃;
DOI:10.1016/S0040-4039(00)73953-0

Reference yield: 20.0%

: 153255-00-6
5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-6-bromo-benzo[1,3]dioxole

: 5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-benzo[1,3]dioxole

: (1S,3aS,10bS)-1-Benzenesulfonyl-1,2,3,3a,5,10b-hexahydro-4,7,9-trioxa-dicyclopenta[a,g]naphthalene

Guidance literature:: With tert.-butyl lithium; In diethyl ether; Yields of byproduct given. Title compound not separated from byproducts; var. solv.: THF;
DOI:10.1016/S0040-4039(00)73953-0

Reference yield: 2.5%

: 153255-00-6
5-(3-Benzenesulfonyl-cyclopent-2-enyloxymethyl)-6-bromo-benzo[1,3]dioxole

: (3aS,10bS)-1-Benzenesulfonyl-3,3a,5,10b-tetrahydro-4,7,9-trioxa-dicyclopenta[a,g]naphthalene

: (1S,3aS,10bS)-1-Benzenesulfonyl-1,3a,5,10b-tetrahydro-4,7,9-trioxa-dicyclopenta[a,g]naphthalene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In acetonitrile; for 1h; Heating;
DOI:10.1016/S0040-4039(00)73953-0