C₅₇H₈₈N₄O₈Si

Base Information

Chemical Name:C₅₇H₈₈N₄O₈Si
CAS No.:173243-78-2
Molecular Formula:C₅₇H₈₈N₄O₈Si
Molecular Weight:985.433
Hs Code.:

C<sub>57</sub>H<sub>88</sub>N<sub>4</sub>O<sub>8</sub>Si

Synonyms:C₅₇H₈₈N₄O₈Si

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Chemical Property of C₅₇H₈₈N₄O₈Si

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Technology Process of C₅₇H₈₈N₄O₈Si

There total 10 articles about C₅₇H₈₈N₄O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120205-58-5
tert-Butyl (3R,4S,5S)-3-methoxy-4--5-methylheptanoate

: 173243-78-2
C₅₇H₈₈N₄O₈Si

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / 10percent Pd/C / methanol / 1.17 h / 760 Torr / Ambient temperature

2: PyBOP, i-Pr₂NEt / CH₂Cl₂ / 17.5 h / 0 - 20 °C

3: H₂ / 10percent Pd/C / methanol / 0.5 h / 760 Torr / Ambient temperature

4: DEPC, Et₃N / dimethylformamide / 2 h / 0 °C

5: TFA / CH₂Cl₂ / 1.5 h / Ambient temperature

6: DEPC, Et₃N / dimethylformamide / 11.17 h / 0 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; diethyl dicarbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja9519086

Reference yield:

: 474645-22-2
tert-Butyl (3R,4S,5S)-3-methoxy-4-(N-methylamino)-5-methylheptanoate

: 173243-78-2
C₅₇H₈₈N₄O₈Si

Guidance literature:: Multi-step reaction with 5 steps

1: PyBOP, i-Pr₂NEt / CH₂Cl₂ / 17.5 h / 0 - 20 °C

2: H₂ / 10percent Pd/C / methanol / 0.5 h / 760 Torr / Ambient temperature

3: DEPC, Et₃N / dimethylformamide / 2 h / 0 °C

4: TFA / CH₂Cl₂ / 1.5 h / Ambient temperature

5: DEPC, Et₃N / dimethylformamide / 11.17 h / 0 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; diethyl dicarbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja9519086

Reference yield:

: 149606-56-4
Cbz-Ile-Dil-O-t-Bu

: 173243-78-2
C₅₇H₈₈N₄O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / methanol / 0.5 h / 760 Torr / Ambient temperature

2: DEPC, Et₃N / dimethylformamide / 2 h / 0 °C

3: TFA / CH₂Cl₂ / 1.5 h / Ambient temperature

4: DEPC, Et₃N / dimethylformamide / 11.17 h / 0 °C

With hydrogen; triethylamine; diethyl dicarbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja9519086