Technology Process of C20H15N3O2
There total 4 articles about C20H15N3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanesulfonic acid;
In
acetonitrile;
at 180 ℃;
for 0.5h;
Microwave irradiation;
DOI:10.1055/s-0032-1317686
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N,N-dimethyl-formamide / dichloromethane
2: ammonia / water; 1,4-dioxane / 20 °C
3: ammonium formate; palladium on activated charcoal; N-ethyl-N,N-diisopropylamine / ethanol / Reflux
4: methanesulfonic acid / acetonitrile / 0.5 h / 180 °C / Microwave irradiation
With
methanesulfonic acid; palladium on activated charcoal; ammonia; ammonium formate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide;
In
1,4-dioxane; ethanol; dichloromethane; water; acetonitrile;
4: |Conrad-Limpach Synthesis;
DOI:10.1055/s-0032-1317686
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium formate; palladium on activated charcoal; N-ethyl-N,N-diisopropylamine / ethanol / Reflux
2: methanesulfonic acid / acetonitrile / 0.5 h / 180 °C / Microwave irradiation
With
methanesulfonic acid; palladium on activated charcoal; ammonium formate; N-ethyl-N,N-diisopropylamine;
In
ethanol; acetonitrile;
2: |Conrad-Limpach Synthesis;
DOI:10.1055/s-0032-1317686
