C₂₇H₄₆O₅Si

Base Information

Chemical Name:C₂₇H₄₆O₅Si
CAS No.:1338704-08-7
Molecular Formula:C₂₇H₄₆O₅Si
Molecular Weight:478.745
Hs Code.:

C<sub>27</sub>H<sub>46</sub>O<sub>5</sub>Si

Synonyms:C₂₇H₄₆O₅Si

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Chemical Property of C₂₇H₄₆O₅Si

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Technology Process of C₂₇H₄₆O₅Si

There total 18 articles about C₂₇H₄₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1338703-90-4
C₂₁H₃₂O₅

: 69739-34-0
t-butyldimethylsiyl triflate

: 1338704-08-7
C₂₇H₄₆O₅Si

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/ol2024289

Reference yield:

: C₁₀H₁₈OS₂

: 1338704-08-7
C₂₇H₄₆O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 25 °C

2.1: tetrahydrofuran; diethyl ether / -78 - 0 °C

3.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

3.2: 1 h / -78 °C

4.1: water; iodine; sodium hydrogencarbonate / acetonitrile / 0.08 h / 0 - 25 °C

5.1: sodium tetrahydroborate; diethyl methoxy borane / tetrahydrofuran; methanol / -78 - 0 °C

6.1: manganese(IV) oxide / dichloromethane / 3 h / 25 °C

7.1: 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; acetic acid / toluene / 72 h / 0 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C

With 2,6-dimethylpyridine; manganese(IV) oxide; sodium tetrahydroborate; 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; diethyl methoxy borane; water; iodine; tert.-butyl lithium; sulfur trioxide pyridine complex; sodium hydrogencarbonate; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; toluene; acetonitrile; pentane;
DOI:10.1021/ol2024289

Reference yield:

: C₁₁H₁₈O₂S₂

: 1338704-08-7
C₂₇H₄₆O₅Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C

2.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 25 °C

3.1: tetrahydrofuran; diethyl ether / -78 - 0 °C

4.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

4.2: 1 h / -78 °C

5.1: water; iodine; sodium hydrogencarbonate / acetonitrile / 0.08 h / 0 - 25 °C

6.1: sodium tetrahydroborate; diethyl methoxy borane / tetrahydrofuran; methanol / -78 - 0 °C

7.1: manganese(IV) oxide / dichloromethane / 3 h / 25 °C

8.1: 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; acetic acid / toluene / 72 h / 0 °C

9.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C

With 2,6-dimethylpyridine; manganese(IV) oxide; sodium tetrahydroborate; 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; diethyl methoxy borane; water; iodine; tert.-butyl lithium; sulfur trioxide pyridine complex; diisobutylaluminium hydride; sodium hydrogencarbonate; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; toluene; acetonitrile; pentane;
DOI:10.1021/ol2024289