ethyl (4S,5S,6R)-4-(benzyloxycarbonylamino)-5-hydroxy-7,7-dimethoxy-6-nitroheptanoate

Base Information

Chemical Name:ethyl (4S,5S,6R)-4-(benzyloxycarbonylamino)-5-hydroxy-7,7-dimethoxy-6-nitroheptanoate
CAS No.:1029289-40-4
Molecular Formula:C₁₉H₂₈N₂O₉
Molecular Weight:428.439
Hs Code.:

Synonyms:ethyl (4S,5S,6R)-4-(benzyloxycarbonylamino)-5-hydroxy-7,7-dimethoxy-6-nitroheptanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (4S,5S,6R)-4-(benzyloxycarbonylamino)-5-hydroxy-7,7-dimethoxy-6-nitroheptanoate

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Technology Process of ethyl (4S,5S,6R)-4-(benzyloxycarbonylamino)-5-hydroxy-7,7-dimethoxy-6-nitroheptanoate

There total 1 articles about ethyl (4S,5S,6R)-4-(benzyloxycarbonylamino)-5-hydroxy-7,7-dimethoxy-6-nitroheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1029289-27-7
(S)-ethyl 4-(benzyloxycarbonylamino)-5-oxopentanoate

: 69425-53-2
2-nitroacetaldehyde dimethyl acetal

: 1029289-40-4
ethyl (4S,5S,6R)-4-(benzyloxycarbonylamino)-5-hydroxy-7,7-dimethoxy-6-nitroheptanoate

Guidance literature:: (S)-ethyl 4-(benzyloxycarbonylamino)-5-oxopentanoate; 2-nitroacetaldehyde dimethyl acetal; With (S)-La-Li₃-(binaphthoxide)3; In tetrahydrofuran; at -50 - -20 ℃; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol800653d