hypho-12-Bn-12,13-CNB₉H₁₅

Base Information

• Chemical Name: hypho-12-Bn-12,13-CNB₉H₁₅
• CAS No.: 179040-76-7
• Molecular Formula: C₈H₂₂B₉N
• Molecular Weight: 229.568
• Mol file: 179040-76-7.mol

Synonyms:hypho-12-Bn-12,13-CNB₉H₁₅

Chemical Property of hypho-12-Bn-12,13-CNB₉H₁₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of hypho-12-Bn-12,13-CNB₉H₁₅

There total 2 articles about hypho-12-Bn-12,13-CNB₉H₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.6%

[PSH]-arachno-7-Bn-7,12-CNB10H13 → hypho-12-Bn-12,13-CNB9H15 (179040-76-7)

Guidance literature:

With H₂SO₄; In dichloromethane; 0°C, stirring (5 h); extraction (2x, CH2Cl2), evapn. (vac. -30°C), addition hexane, filtration, evapn. (vac. -30°C), recrystn. (CH2Cl2/hexane); elem. anal.;

DOI:10.1021/ja960787m

Reference yield:

[PSH] hypho-12Bn-12,13-CNB9H14 → hypho-12-Bn-12,13-CNB9H15 (179040-76-7)

Guidance literature:

With 1.0 M HCl/Et₂O; In dichloromethane; not isolated;

DOI:10.1021/ja960787m

Reference yield: 100.0%

hypho-12-Bn-12,13-CNB9H15 (179040-76-7) + N,N,N',N'-tetramethyl-1,8-diaminonaphthalene (20734-58-1) → [PSH] hypho-12Bn-12,13-CNB9H14

Guidance literature:

In dichloromethane; stirring (5 min); pptn. (hexane), washing (hexane), drying (vac., 1 h);

DOI:10.1021/ja960787m

Downstream raw materials:

hypho-8-Bn-8,13-CNB₈H₁₄