Technology Process of [4-(6-Benzyloxy-naphthalen-2-yloxy)-phenyl]-acetyl chloride
There total 4 articles about [4-(6-Benzyloxy-naphthalen-2-yloxy)-phenyl]-acetyl chloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxalyl dichloride;
In
dichloromethane;
at 35 ℃;
for 1h;
DOI:10.1021/jm9605041
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) NaOMe, 2.) CuCl / 1.) MeOH, benzene, RT, 1 h, 2.) pyridine, 120 deg C, 86 h
2: 4N aq. LiOH / methanol; tetrahydrofuran / Ambient temperature
3: oxalyl chloride / CH2Cl2 / 1 h / 35 °C
With
lithium hydroxide; oxalyl dichloride; sodium methylate; copper(l) chloride;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm9605041
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) NaOMe, 2.) CuCl / 1.) MeOH, benzene, RT, 1 h, 2.) pyridine, 120 deg C, 86 h
2: 4N aq. LiOH / methanol; tetrahydrofuran / Ambient temperature
3: oxalyl chloride / CH2Cl2 / 1 h / 35 °C
With
lithium hydroxide; oxalyl dichloride; sodium methylate; copper(l) chloride;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm9605041
