2,2,10,10-tetramethyl-1⁴,11⁴-di(tetrahydropyran-2-yloxy)-4,8-dioxa-6²-aza-1,3(1,4),6(1,3),9(1,4),11-pentabenzenaundecaphane

Base Information

• Chemical Name: 2,2,10,10-tetramethyl-1⁴,11⁴-di(tetrahydropyran-2-yloxy)-4,8-dioxa-6²-aza-1,3(1,4),6(1,3),9(1,4),11-pentabenzenaundecaphane
• CAS No.: 161092-73-5
• Molecular Formula: C₄₇H₅₃NO₆
• Molecular Weight: 727.941

Synonyms:2,2,10,10-tetramethyl-1⁴,11⁴-di(tetrahydropyran-2-yloxy)-4,8-dioxa-6²-aza-1,3(1,4),6(1,3),9(1,4),11-pentabenzenaundecaphane

Chemical Property of 2,2,10,10-tetramethyl-1⁴,11⁴-di(tetrahydropyran-2-yloxy)-4,8-dioxa-6²-aza-1,3(1,4),6(1,3),9(1,4),11-pentabenzenaundecaphane

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Technology Process of 2,2,10,10-tetramethyl-1⁴,11⁴-di(tetrahydropyran-2-yloxy)-4,8-dioxa-6²-aza-1,3(1,4),6(1,3),9(1,4),11-pentabenzenaundecaphane

There total 1 articles about 2,2,10,10-tetramethyl-1⁴,11⁴-di(tetrahydropyran-2-yloxy)-4,8-dioxa-6²-aza-1,3(1,4),6(1,3),9(1,4),11-pentabenzenaundecaphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2,6-bis-(bromomethyl)pyridine (7703-74-4) + 4-(2-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)propan-2-yl)phenol (23359-00-4) → 2,2,10,10-tetramethyl-14,114-di(tetrahydropyran-2-yloxy)-4,8-dioxa-62-aza-1,3(1,4),6(1,3),9(1,4),11-pentabenzenaundecaphane (161092-73-5)

Guidance literature:

With potassium carbonate; In ethanol; for 20h; Heating;

Reference yield: 96.0%

2,2,10,10-tetramethyl-14,114-di(tetrahydropyran-2-yloxy)-4,8-dioxa-62-aza-1,3(1,4),6(1,3),9(1,4),11-pentabenzenaundecaphane (161092-73-5) → 2,2,10,10-tetramethyl-4,8-dioxa-62-aza-1,3(1,4),6(1,3),9(1,4),11-pentabenzenaundecaphane-14,114-diol

Guidance literature:

With hydrogenchloride; In methanol; chloroform; Heating;

upstream raw materials:

2,6-bis-(bromomethyl)pyridine

4-(2-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)propan-2-yl)phenol

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