(1R,3R,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-1-hydroxymethyl-cyclohexane-1,3-diol

Base Information

Chemical Name:(1R,3R,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-1-hydroxymethyl-cyclohexane-1,3-diol
CAS No.:439814-54-7
Molecular Formula:C₁₉H₄₂O₅Si₂
Molecular Weight:406.71
Hs Code.:

Synonyms:(1R,3R,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-1-hydroxymethyl-cyclohexane-1,3-diol

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Chemical Property of (1R,3R,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-1-hydroxymethyl-cyclohexane-1,3-diol

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Technology Process of (1R,3R,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-1-hydroxymethyl-cyclohexane-1,3-diol

There total 4 articles about (1R,3R,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-1-hydroxymethyl-cyclohexane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₄₀H₆₀O₅Si₂

: 439814-54-7
(1R,3R,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-1-hydroxymethyl-cyclohexane-1,3-diol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1039/b200624c

Reference yield:

: 35949-54-3
(1R,2S,3R,5R)-1,2-O-cyclohexylidene-5-C-(hydroxymethyl)-1,2,3,5-cyclohexanetetrol

: 439814-54-7
(1R,3R,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-1-hydroxymethyl-cyclohexane-1,3-diol

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / NaH / dimethylformamide

2: 95 percent / aq. AcOH / 10 h / 50 °C

3: 80 percent / ImH; DMAP / dimethylformamide / 24 °C

4: 100 percent / H₂ / Pd/C / ethanol

With 1H-imidazole; dmap; hydrogen; sodium hydride; acetic acid; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/b200624c

Reference yield:

: C₃₄H₄₀O₅

: 439814-54-7
(1R,3R,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-1-hydroxymethyl-cyclohexane-1,3-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / aq. AcOH / 10 h / 50 °C

2: 80 percent / ImH; DMAP / dimethylformamide / 24 °C

3: 100 percent / H₂ / Pd/C / ethanol

With 1H-imidazole; dmap; hydrogen; acetic acid; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/b200624c