Technology Process of 5-(4-isopropylphenyl)imidazo[1,2-f]phenanthridine
There total 6 articles about 5-(4-isopropylphenyl)imidazo[1,2-f]phenanthridine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium diacetate; potassium carbonate; triphenylphosphine;
In
1,2-dimethoxyethane; water;
at 80 ℃;
for 17h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bis-triphenylphosphine-palladium(II) chloride; potassium phosphate monohydrate / toluene / 6 h / 100 °C / Inert atmosphere
2: sodium hydrogencarbonate / water; isopropyl alcohol / 5 h / 75 °C
3: potassium carbonate; palladium diacetate; triphenylphosphine / water; 1,2-dimethoxyethane / 17 h / 80 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate monohydrate; palladium diacetate; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine;
In
1,2-dimethoxyethane; water; isopropyl alcohol; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydrogencarbonate / water; isopropyl alcohol / 5 h / 75 °C
2: potassium carbonate; palladium diacetate; triphenylphosphine / water; 1,2-dimethoxyethane / 17 h / 80 °C / Inert atmosphere
With
palladium diacetate; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine;
In
1,2-dimethoxyethane; water; isopropyl alcohol;