N,N-dimethyl alpha-(2-oxo 2,4,5,6,7,7a-hexahydro thieno [3,2-c] 5-pyridyl) (2-chloro phenyl)-acetamide

Base Information

Chemical Name:N,N-dimethyl alpha-(2-oxo 2,4,5,6,7,7a-hexahydro thieno [3,2-c] 5-pyridyl) (2-chloro phenyl)-acetamide
CAS No.:109904-35-0
Molecular Formula:C₁₇H₁₉ClN₂O₂S
Molecular Weight:350.869
Hs Code.:

Synonyms:N,N-dimethyl alpha-(2-oxo 2,4,5,6,7,7a-hexahydro thieno [3,2-c] 5-pyridyl) (2-chloro phenyl)-acetamide

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Chemical Property of N,N-dimethyl alpha-(2-oxo 2,4,5,6,7,7a-hexahydro thieno [3,2-c] 5-pyridyl) (2-chloro phenyl)-acetamide

Chemical Property:

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Technology Process of N,N-dimethyl alpha-(2-oxo 2,4,5,6,7,7a-hexahydro thieno [3,2-c] 5-pyridyl) (2-chloro phenyl)-acetamide

There total 4 articles about N,N-dimethyl alpha-(2-oxo 2,4,5,6,7,7a-hexahydro thieno [3,2-c] 5-pyridyl) (2-chloro phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 109904-35-0
N,N-dimethyl alpha-(2-oxo 2,4,5,6,7,7a-hexahydro thieno [3,2-c] 5-pyridyl) (2-chloro phenyl)-acetamide

Guidance literature:

Reference yield:

: 109904-37-2
5,6,7,7a-tetrahydrothieno[3,2-c]pyridine-2(4H)-one monohydrochloride

: C₁₇H₁₈ClNO₄S

: 109904-35-0
N,N-dimethyl alpha-(2-oxo 2,4,5,6,7,7a-hexahydro thieno [3,2-c] 5-pyridyl) (2-chloro phenyl)-acetamide

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 24h;

Reference yield:

: C₁₀H₁₂ClNO₂

: 109904-35-0
N,N-dimethyl alpha-(2-oxo 2,4,5,6,7,7a-hexahydro thieno [3,2-c] 5-pyridyl) (2-chloro phenyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 h / 20 °C / Cooling with ice

2: potassium carbonate / acetonitrile / 24 h / 20 °C

With potassium carbonate; triethylamine; In dichloromethane; acetonitrile;