(S_p)-N-methyl-N-[(-)-menthyloxy(4-methoxyphenyl)phosphinothioyloxy]-4-chlorobenzamide

Base Information

• Chemical Name: (S_p)-N-methyl-N-[(-)-menthyloxy(4-methoxyphenyl)phosphinothioyloxy]-4-chlorobenzamide
• CAS No.: 1144028-87-4
• Molecular Formula: C₂₅H₃₃ClNO₄PS
• Molecular Weight: 510.034

Synonyms:(S_p)-N-methyl-N-[(-)-menthyloxy(4-methoxyphenyl)phosphinothioyloxy]-4-chlorobenzamide

Chemical Property of (S_p)-N-methyl-N-[(-)-menthyloxy(4-methoxyphenyl)phosphinothioyloxy]-4-chlorobenzamide

Chemical Property:

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Technology Process of (S_p)-N-methyl-N-[(-)-menthyloxy(4-methoxyphenyl)phosphinothioyloxy]-4-chlorobenzamide

There total 1 articles about (S_p)-N-methyl-N-[(-)-menthyloxy(4-methoxyphenyl)phosphinothioyloxy]-4-chlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(Rp,Rp)-bis[(-)-menthyloxy(4-methoxyphenyl)-phosphinothioyl]disulfane + N-methyl-4-chlorobenzohydroxamic acid sodium salt (123381-62-4) → (Sp)-N-methyl-N-[(-)-menthyloxy(4-methoxyphenyl)phosphinothioyloxy]-4-chlorobenzamide (1144028-87-4) + C17H26O2PS2(1-)*Na(1+) (1144028-88-5)

Guidance literature:

N-methyl-4-chlorobenzohydroxamic acid sodium salt; With sodium hydride; In tetrahydrofuran; for 1.5h; Heating;

(R_p,R_p)-bis[(-)-menthyloxy(4-methoxyphenyl)-phosphinothioyl]disulfane; In tetrahydrofuran; at 20 ℃; for 0.333333h; Further stages.;

DOI:10.1002/hc.20423

upstream raw materials:

N-methyl-4-chlorobenzohydroxamic acid sodium salt

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