Technology Process of C54H93N3O6Si3
There total 9 articles about C54H93N3O6Si3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: CH2Cl2
2: 83 percent / t-BuOK / tetrahydrofuran
3: 73 percent / t-BuOK; 18-crown-6 / tetrahydrofuran
With
18-crown-6 ether; potassium tert-butylate;
In
tetrahydrofuran; dichloromethane;
2: retro-Michael reaction;
DOI:10.1016/j.tetlet.2004.08.160
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 90 percent / t-BuOK / tetrahydrofuran
2.1: 9-BBN / tetrahydrofuran
2.2: 100 percent / H2O2; NaOH / tetrahydrofuran; H2O
3.1: 72 percent / NaH / tetrahydrofuran
4.1: NBS; AIBN / hexane
5.1: γ-collidine / toluene
6.1: CH2Cl2
7.1: 83 percent / t-BuOK / tetrahydrofuran
8.1: 73 percent / t-BuOK; 18-crown-6 / tetrahydrofuran
With
2,4,6-trimethyl-pyridine; N-Bromosuccinimide; 9-borabicyclo[3.3.1]nonane dimer; 18-crown-6 ether; 2,2'-azobis(isobutyronitrile); potassium tert-butylate; sodium hydride;
In
tetrahydrofuran; hexane; dichloromethane; toluene;
1.1: Wittig reaction / 3.1: Michael reaction / 7.1: retro-Michael reaction;
DOI:10.1016/j.tetlet.2004.08.160