1-(4-Methoxy-benzyloxymethoxy)-3,3-dimethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

Base Information

Chemical Name:1-(4-Methoxy-benzyloxymethoxy)-3,3-dimethyl-2,3,3a,4,5,7a-hexahydro-1H-indene
CAS No.:118617-80-4
Molecular Formula:C₂₀H₂₈O₃
Molecular Weight:316.441
Hs Code.:

Synonyms:1-(4-Methoxy-benzyloxymethoxy)-3,3-dimethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

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Chemical Property of 1-(4-Methoxy-benzyloxymethoxy)-3,3-dimethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

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Technology Process of 1-(4-Methoxy-benzyloxymethoxy)-3,3-dimethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

There total 3 articles about 1-(4-Methoxy-benzyloxymethoxy)-3,3-dimethyl-2,3,3a,4,5,7a-hexahydro-1H-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 118617-78-0
3,3-Dimethyl-2,3,3a,4,5,7a-hexahydro-1H-inden-1-ol

: 88023-78-3
para-methoxybenzyl chloride

: 118617-80-4
1-(4-Methoxy-benzyloxymethoxy)-3,3-dimethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1016/S0040-4039(00)95608-9

Reference yield:

: 53942-86-2
4-methoxybenzyl alcohol sodium salt

: 118617-80-4
1-(4-Methoxy-benzyloxymethoxy)-3,3-dimethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

Guidance literature:: Multi-step reaction with 3 steps

2: sulfuryl chloride / CH₂Cl₂ / -78 °C

3: 96 percent / diisopropylethylamine / CH₂Cl₂ / 4 h / Ambient temperature

With sulfuryl dichloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)95608-9

Reference yield:

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 118617-80-4
1-(4-Methoxy-benzyloxymethoxy)-3,3-dimethyl-2,3,3a,4,5,7a-hexahydro-1H-indene

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl chloride / CH₂Cl₂ / -78 °C

2: 96 percent / diisopropylethylamine / CH₂Cl₂ / 4 h / Ambient temperature

With sulfuryl dichloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)95608-9