(2S)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylic acid

Base Information

• Chemical Name: (2S)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylic acid
• CAS No.: 305836-78-6
• Molecular Formula: C₁₃H₁₅NO₄S
• Molecular Weight: 281.332

Synonyms:(2S)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylic acid

Chemical Property of (2S)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylic acid

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of (2S)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylic acid

There total 11 articles about (2S)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

[1-(toluene-4-sulfonyl)-1,2,3,6-tetrahydro-pyridin-2-yl]-methanol (919116-91-9) → (2S)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylic acid (305836-78-6)

Guidance literature:

With jones reagent; In acetone; at 20 ℃; for 0.333333h;

DOI:10.3987/COM-06-10874

Reference yield: 70.0%

1,2,3,6-tetrahydropyridine-2-carboxylic acid hydrochloride (76472-92-9) + p-toluenesulfonyl chloride (98-59-9) → (2S)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylic acid (305836-78-6)

Guidance literature:

With sodium hydroxide; at 20 ℃; for 17h;

DOI:10.1002/1099-0690(200207)2002:14<2308::AID-EJOC2308<3.0.CO;2-Q

Reference yield: 68.0%

poly(ethylene glycol)-3400 di((L)-N-tosyl-4,5-didehydropipecolate) → (2S)-1-(4-methylphenylsulfonyl)-1,2,3,6-tetrahydropyridine-2-carboxylic acid (305836-78-6)

Guidance literature:

With hydrogenchloride; for 4h; Heating;

DOI:10.1021/jo000898a

upstream raw materials:

1,2,3,6-tetrahydropyridine-2-carboxylic acid hydrochloride

p-toluenesulfonyl chloride

[1-(toluene-4-sulfonyl)-1,2,3,6-tetrahydro-pyridin-2-yl]-methanol

N-allyl-N-(1-benzyloxymethyl-3-oxopropyl)-4-methylbenzenesulfonamide

Downstream raw materials:

(2S)-1,2,3,6-tetrahydropyridine-2-carboxylic acid

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